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Solvent Reports
This may be useful for some chemists: http://www.salvia-info.com/lab/solv...orts/#everclear ---------------------------------------------------------
Acetone Synonyms - Dimethyl Ketone Formula - CH3 CO CH3 B.P. - 56.5º C Density - .792 g/ml MSDS
Klean Strip® Acetone Address: www.kleanstrip.com Purchased: 1 qt can At: hardware store - paint section Amount distilled: 500 ml Results: 30-35° aprox 5 ml unable to identify 57° 485ml Acetone last 10 ml evaporated. Left oily residue that smelled 'industrial' like compressor oil Rating: GOOD - Should distill first
Zip-Strip Acetone Address:http://www.starbronze.com Purchased:1 Gal. Can At: Sears Hardware Store - may be discontinued soon Amount Distilled:800ml Results: Very Clean!! The cleanest I have tested so far. Of course your can could differ and you should distill anyway. Last 5 ml evaporated for residue check. Approx. last 1 ml was aromatic but evaporated. About 1 drop of oily residue was left. Rating: VERY GOOD - Should distill first
Methyl Ethyl Ketone Synonyms - MEK, 2-Butanone Formula - CH3 CO C2H5 B.P. - 79.6º C Density - .805 g/ml MSDS
Zip-Strip MEK Address:http://www.starbronze.com Purchased:1 Qt Can At:Sears Hardware Store Amount Distilled:1 Qt. Results: With about 50ml left, color started to get darker (brownish red). Temperature started to rise with about 10ml left. Water azeotrope boils lower so it was something else. Last 8ml evaporated. At 5ml it was almost all aromatic (Toluene?). Left about 5 drops oily reddish residue. Rating: Good - Must distill first
Petroleum Ether Synonyms - Petroleum Spirits, Petroleum Distillates, Ligroine Formula - N/A (Mixture of compounds) B.P. 20-80º Density - N/A MSDS
Ozark Trail® Camp Fuel Address: Purchased:1 Gal Can At: Wal-Mart Amount Distilled: 1500 ml Results: 35° aprox 50 ml (probably n-Penatne) 69° aprox 1000 ml (probably n-Hexane) 74° aprox 200 ml 80-120° aprox 250 ml Last 3-5 ml would not distill. Solidified to Vaseline like grease upon cooling Rating: GOOD - Should distill first
Coleman® Lantern Fuel Address:www.coleman.com Purchased:1 Gallon Can At:Camping Store - $4.98 Amount Distilled:100ml Results: 69° Aprox 10 ml Hexane - smelled perfumy Rest was higher fractions Left dark blue/green oil which solidified to Vaseline consistency on cooling Rating: POOR - Do not use
Ronsonol® Lighter Fluid Address:Woodbridge, NJ Purchased:12 oz. bottle At:Grocery Store - $3.69 Amount Distilled:- Results: Had a yellow tint - possibly from the bottle 115° First fraction started Due to high b.p. I did not continue Rating: POOR Due to high b.p. would be hard to evaporate to dryness
Klean Strip® V,M&P Naphtha Address: www.kleanstrip.com Purchased:1 Qt. Can At:Hardware Store - Paint section Amount Distilled:- Results: No fraction until 130º - Didn't bother Rating: POOR Due to high b.p. would be hard to evaporate to dryness
Methyl Alcohol Synonyms - Methanol, Wood Alcohol Formula - CH3 OH B.P. - 64.7º C Density - .792 g/ml MSDS
HEET® Gas Line Antifreeze Address:www.goldeagle.com Purchased:4 Pack of 12oz bottles At:Walmart - $3.59 Amount Distilled:500 ml Results: Methyl Alcohol distilled over nicely Last 10 ml evaporated left slightly oily residue Rating: GOOD - Should distill first
Ethyl Alcohol Synonyms - Ethanol, Grain Alcohol Formula - CH3 CH2 OH B.P. - 78.5º C (95% azeotrope - 78.2°) Density - .789 g/ml MSDS
Everclear® Grain Alcohol Address:? Purchased:750 ml At:Liquor Store / mail order Amount Distilled:N/A Results: Does not need to be distilled Rating: Excelent - Use for tinctures
Klean Strip® Denatured Alcohol Address: www.kleanstrip.com Purchased:1 qt. Can At:Hardware Store - Paint section Amount Distilled:1 qt. Results: Distills over nicely Left oily residue Rating: GOOD - Should distill first ***DO NOT USE FOR TINCTURES - Must be fully evaporated from final product | | Reply » Solvent Reports |
how do you "distill" acetone?
| | Reply » Solvent Reports |
You need lab equipment, but what you do is heat it up, let it evaporate but then collect the vapor and condense it into another container. The liquid you have in your container is not a much purer acetone.
| | Reply » Solvent Reports |
i think you would be able to do it without lab equipment, like on of those home distillers for making your own beer you see in places, or just make your one, if its worht it to you
| | Reply » Solvent Reports |
Ya you can, Ive done it many of times. It just helps to know exactly how they work and what they look like. All you need is like a beaker, a funnel, a tube and another beaker.
Take one beaker and put your solvent in it.
Attach the tube to the funnel. Place the funnel upside down on the solvent beaker and seal it up. It now looks like a rocket with like a hose sticking out of it lol.
Take the other end of the hose and stick it in your empty beaker.
Now heat up your solvent one. As it heats and eveaporates, it will transfer. Keep an eye on the temperature, it should stay withing 10 degrees of what your usings BP.
| | Reply » Solvent Reports |
With acetone distillation try not to heat rapidly (more than 1 degree / 5 minutes). Also, do not use open flames for a source of heat but instead use an oil bath with a fine temperature control...unless, of course, you intended on redecorating the kitchen anyway.  Chemo
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